(1-methoxy-1-iodo-2-methylpropyl)triethylphosphonium iodide

Base Information

• Chemical Name: (1-methoxy-1-iodo-2-methylpropyl)triethylphosphonium iodide
• CAS No.: 76047-26-2
• Molecular Formula: C₁₁H₂₅IOP*I
• Molecular Weight: 458.102
• Mol file: 76047-26-2.mol

Synonyms:

Chemical Property of (1-methoxy-1-iodo-2-methylpropyl)triethylphosphonium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1-methoxy-1-iodo-2-methylpropyl)triethylphosphonium iodide

There total 1 articles about (1-methoxy-1-iodo-2-methylpropyl)triethylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O-methyl selenoisobutirate (76047-09-1) + triethylphosphine (554-70-1) → trimethylselenonium iodide (7362-34-7) + (1-methoxy-1-iodo-2-methylpropyl)triethylphosphonium iodide (76047-26-2)

Guidance literature:

With sodium iodide; methyl iodide; Yield given. Multistep reaction; 1.) benzene, 50 deg C, 5 h, 2.) tetrahydrofuran, 15 min;

Reference yield:

benzaldehyde (100-52-7) + (1-methoxy-1-iodo-2-methylpropyl)triethylphosphonium iodide (76047-26-2) → isobutyroin (815-77-0) + triethylmethylphosphonium iodide (7017-05-2) + 1-phenyl-2-methoxy-3-methylbutan-1-one (76047-14-8)

Guidance literature:

With methyl iodide; Yield given. Multistep reaction. Yields of byproduct given; 1.) tetrahydrofuran, -70 deg C, 1 h, 2.) 15 min;

upstream raw materials:

O-methyl selenoisobutirate

triethylphosphine

Downstream raw materials:

isobutyroin

triethylmethylphosphonium iodide

1-phenyl-2-methoxy-3-methylbutan-1-one

Refernces