PhenDC3

Base Information

• Chemical Name: PhenDC3
• CAS No.: 929895-45-4
• Molecular Formula: 2CF₃O₃S*C₃₄H₂₆N₆O₂
• Molecular Weight: 848.76
• Mol file: 929895-45-4.mol

Synonyms:

Chemical Property of PhenDC3

Chemical Property:

• Melting Point: >260 °C(Solv: ethyl ether (60-29-7))

Purity/Quality:

99% ^*data from raw suppliers

Phen-DC3Trifluoromethanesulfonate 99.53% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of PhenDC3

There total 6 articles about PhenDC3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N-bis(3-[1-methylquinolinium])-1,10-phenanthroline-2,9-dicarboxamide diiodide + silver trifluoromethanesulfonate (2923-28-6) → PhenDC3 (929895-45-4)

Guidance literature:

In methanol; acetonitrile; at 20 ℃; for 0.5h; Darkness;

DOI:10.1055/s-0036-1591994

Reference yield: 84.0%

N,N-bis(3-[1-methylquinolinium])-1,10-phenanthroline-2,9-dicarboxamide diiodide + calcium(II) trifluoromethanesulfonate (55120-75-7) → PhenDC3 (929895-45-4)

Guidance literature:

In methanol; acetonitrile; at 20 ℃; for 0.666667h; Darkness;

DOI:10.1055/s-0036-1591994

Reference yield: 50.0%

N2,N9-di(quinolin-3-yl)-1,10-phenanthroline-2,9-dicarboxamide (929895-49-8) + methyl trifluoromethanesulfonate (333-27-7) → PhenDC3 (929895-45-4)

Guidance literature:

In 1,2-dichloro-ethane; Heating;

DOI:10.1021/ja067352b

upstream raw materials:

N²,N⁹-di(quinolin-3-yl)-1,10-phenanthroline-2,9-dicarboxamide

methyl trifluoromethanesulfonate

2.9-dimethyl-1,10-phenanthroline

1,10-phenanthroline-2,9-dicarboxaldehyde

Refernces

• 1、 De Cian, Anne,DeLemos, Elsa,Mergny, Jean-Louis,Teulade-Fichou, Marie-Paule,Monchaud, David. "Highly efficient G-quadruplex recognition by bisquinolinium compounds". . p. 1856 - 1857. Retrieved 2008/01/27.