diamantane-1,6-diol

Base Information

• Chemical Name: diamantane-1,6-diol
• CAS No.: 62297-03-4
• Molecular Formula: C₁₄H₂₀O₂
• Molecular Weight: 220.312
• Mol file: 62297-03-4.mol

Synonyms:

Chemical Property of diamantane-1,6-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diamantane-1,6-diol

There total 3 articles about diamantane-1,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,6-dibromodiamantane (32401-10-8) → diamantane-1,6-diol (62297-03-4)

Guidance literature:

With nitric acid; at 70 ℃; for 0.333333h;

Reference yield:

diamantane (2292-79-7) → diamantane-1,6-diol (62297-03-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.8 g / Bromine / 1.) R_.T_., 2.) reflux, 18 h.

2: 68 percent / 65percent HNO₃ / 0.33 h / 70 °C

With bromine; nitric acid;

Reference yield:

diamantane (2292-79-7) → diamantane-1,6-diol (62297-03-4) + MDT-14 (39646-84-9) + diamantane-1,4-diol (77076-31-4)

Guidance literature:

With aluminum tri-bromide; bromine; nitric acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) -7 deg C, 3 min, 2.) 20 min.;

upstream raw materials:

diamantane

1,6-dibromodiamantane

Refernces

• 1、 Vodicka, Ludek,Janku, Josef,Burkhard, Jiri. "SYNTHESIS OF DIAMANTANEDICARBOXYLIC ACIDS WITH THE CARBOXY GROUPS BONDED AT TERTIARY CARBON ATOMS". . p. 1162 - 1172. Retrieved 2007/10/02.