Technology Process of 1-(2'-fluoro-4''-propyl[1,1':4',1''-terphenyl]-4-yl)-1-pentanone
There total 8 articles about 1-(2'-fluoro-4''-propyl[1,1':4',1''-terphenyl]-4-yl)-1-pentanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
aluminium trichloride;
In
nitrobenzene;
for 16h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: magnesium turnings / diethyl ether / 0.5 h / Heating
2: diethyl ether / 0.5 h / Heating
3: phosphorus pentoxide / benzene / 3.5 h / Ambient temperature
4: 2,3-dichloro-5,6-dicyanobenzoquinone / toluene / 3 h / 110 °C
5: 48 percent / anhydrous aluminium chloride / nitrobenzene / 16 h / Ambient temperature
With
phosphorus pentaoxide; aluminium trichloride; magnesium; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
diethyl ether; nitrobenzene; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethyl ether / 0.5 h / Heating
2: phosphorus pentoxide / benzene / 3.5 h / Ambient temperature
3: 2,3-dichloro-5,6-dicyanobenzoquinone / toluene / 3 h / 110 °C
4: 48 percent / anhydrous aluminium chloride / nitrobenzene / 16 h / Ambient temperature
With
phosphorus pentaoxide; aluminium trichloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
diethyl ether; nitrobenzene; toluene; benzene;