O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate

Base Information

• Chemical Name: O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate
• CAS No.: 74752-32-2
• Molecular Formula: C₁₃H₁₈N₂O₃S
• Molecular Weight: 282.364
• Mol file: 74752-32-2.mol

Synonyms:

Chemical Property of O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate

There total 1 articles about O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-tert-butyl-2-nitrophenol (3279-07-0) + N,N-Dimethylthiocarbamoyl chloride (16420-13-6) → O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate (74752-32-2)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction;

DOI:10.1021/jo01309a030

Reference yield:

O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate (74752-32-2) → 4-tert-Butyl-2-nitrothiophenol (74752-38-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Heating

2: 79 percent / K₂CO₃

With potassium carbonate;

DOI:10.1021/jo01309a030

Reference yield:

O-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate (74752-32-2) → 4-tert-Butyl-2-nitrobenzenesulfenyl Chloride (74752-41-3)

Guidance literature:

Multi-step reaction with 3 steps

1: Heating

2: 79 percent / K₂CO₃

3: 99 percent / SO₂Cl₂

With sulfuryl dichloride; potassium carbonate;

DOI:10.1021/jo01309a030

upstream raw materials:

4-tert-butyl-2-nitrophenol

N,N-Dimethylthiocarbamoyl chloride

Downstream raw materials:

S-4-tert-Butyl-2-nitrophenyl Dimethylcarbamothioate

4-tert-Butyl-2-nitrothiophenol

4-tert-Butyl-2-nitrobenzenesulfenyl Chloride

β-D-Glucopyranosyl 4-tert-Butyl-2-nitrophenyl Disulfide

Refernces