(2R^,4aS^,5S^,8aR^)-2-(1-propyl)-5-methyldecahydroquinoline hydrochloride

Base Information Edit

Chemical Name:(2R^*,4aS^*,5S^*,8aR^*)-2-(1-propyl)-5-methyldecahydroquinoline hydrochloride
CAS No.:55785-30-3
Molecular Formula:C₁₃H₂₅N*ClH
Molecular Weight:231.809
Hs Code.:
Mol file:55785-30-3.mol

(2R<sup>*</sup>,4aS<sup>*</sup>,5S<sup>*</sup>,8aR<sup>*</sup>)-2-(1-propyl)-5-methyldecahydroquinoline hydrochloride

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R^*,4aS^*,5S^*,8aR^*)-2-(1-propyl)-5-methyldecahydroquinoline hydrochloride Edit

Chemical Property:

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Technology Process of (2R^*,4aS^*,5S^*,8aR^*)-2-(1-propyl)-5-methyldecahydroquinoline hydrochloride

There total 12 articles about (2R^*,4aS^*,5S^*,8aR^*)-2-(1-propyl)-5-methyldecahydroquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 142003-59-6
(2S^*,4aS^*,5S^*,8aR^*)-1-benzyl-2-(1-propyl)-(Δ-3,4)-5-methyl-(Δ-6,7)-7-<(trifluoromethanesulfonyl)oxy>hexahydroquinoline

: 55785-30-3
(+/-)-pumiliotoxine C hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 20h; under 760 Torr;
DOI:10.1021/jo00041a012

Reference yield:

: 142003-72-3
(2S,4aS,8aR)-1-Benzyl-2-propyl-2,4a,8,8a-tetrahydro-1H-quinolin-7-one

: 55785-30-3
(+/-)-pumiliotoxine C hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1) THF, a) -78 deg C, 45 min, b) 0 deg C, 35 min, 2) THF, a) 0 deg C, 2 h, b) r.t., 1 h

2: 60 percent / H₂ / 10percent Pd/C / methanol / 20 h / 760 Torr

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00041a012

Reference yield:

: (±)-N-hydroxy-(2R*,4aS*,5R*,8aR*)-decahydro-5-methyl-2-propylquinoline

: 55785-30-3,58117-91-2,61424-98-4,87037-33-0,87517-37-1,95534-64-8
(2R^*,4aS^*,5S^*,8aR^*)-2-(1-propyl)-5-methyldecahydroquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; acetic acid / water / 4 h / 55 °C

2: hydrogenchloride / methanol / 0.42 h

With hydrogenchloride; acetic acid; zinc; In methanol; water;
DOI:10.1021/jo4023149