(R,R)-2,5-diacetoxyhexane

Base Information

• Chemical Name: (R,R)-2,5-diacetoxyhexane
• CAS No.: 97100-83-9
• Molecular Formula: C₁₀H₁₈O₄
• Molecular Weight: 202.251
• Mol file: 97100-83-9.mol

Synonyms:

Chemical Property of (R,R)-2,5-diacetoxyhexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R,R)-2,5-diacetoxyhexane

There total 1 articles about (R,R)-2,5-diacetoxyhexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-2,5-hexanediol (38484-56-9) + 4-chlorophenyl acetate (876-27-7) → (2R,5R)-2,5-hexanediol (17299-07-9) + (R,R)-2,5-diacetoxyhexane (97100-83-9) + (2S,5S)-2,5-hexanediol (34338-96-0) + (2R,5R)-5-acetoxy-2-hexanol (475051-22-0)

Guidance literature:

Candida antarctica lipase B; In toluene; at 20 ℃; for 0.0416667h; Title compound not separated from byproducts;

DOI:10.1002/chem.200600257

Reference yield: 100.0%

(R,R)-2,5-diacetoxyhexane (97100-83-9) → (2R,5R)-2,5-hexanediol (17299-07-9)

Guidance literature:

With lithium hydroxide; In methanol; at 25 ℃; for 8h;

DOI:10.1021/jo00075a056

upstream raw materials:

(+/-)-2,5-hexanediol

4-chlorophenyl acetate

Downstream raw materials:

(2R,5R)-2,5-hexanediol

Refernces