3-(4-amino-phenyl)-[5]quinolylamine

Base Information

• Chemical Name: 3-(4-amino-phenyl)-[5]quinolylamine
• CAS No.: 101101-67-1
• Molecular Formula: C₁₅H₁₃N₃
• Molecular Weight: 235.288
• Mol file: 101101-67-1.mol

Synonyms:

Chemical Property of 3-(4-amino-phenyl)-[5]quinolylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-amino-phenyl)-[5]quinolylamine

There total 10 articles about 3-(4-amino-phenyl)-[5]quinolylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-nitro-3-(4-nitro-phenyl)-quinoline (108062-00-6) → 3-(4-amino-phenyl)-[5]quinolylamine (101101-67-1)

Guidance literature:

With hydrogenchloride; tin(ll) chloride;

DOI:10.1021/jo01096a031

Reference yield:

3-methylquinoline (612-58-8) → 3-(4-amino-phenyl)-[5]quinolylamine (101101-67-1)

Guidance literature:

Multi-step reaction with 10 steps

1: concentrated sulfuric acid; nitric acid

2: CrO₃; MnO₂; aqueous H₂SO₄

3: SOCl₂ / Behandeln des Reaktionsprodukts mit wss. NaN₃ in Aceton

5: aqueous HCl / Erwaermen des Reaktionsprodukts mit Acetanhydrid in Benzol

6: aqueous HCl

7: HCl; NaNO₂; Na₂CO₃

8: benzene; toluene-4-sulfonic acid

9: sulfuric acid; nitric acid

10: SnCl₂; concentrated aqueous HCl

With chromium(VI) oxide; hydrogenchloride; manganese(IV) oxide; thionyl chloride; sulfuric acid; nitric acid; sodium carbonate; toluene-4-sulfonic acid; tin(ll) chloride; sodium nitrite; benzene;

DOI:10.1021/jo01096a031

Reference yield:

3-phenylquinoline (1666-96-2) → 3-(4-amino-phenyl)-[5]quinolylamine (101101-67-1)

Guidance literature:

Multi-step reaction with 3 steps

1: concentrated sulfuric acid; nitric acid

2: sulfuric acid; nitric acid

3: SnCl₂; concentrated aqueous HCl

With hydrogenchloride; sulfuric acid; nitric acid; tin(ll) chloride;

DOI:10.1021/jo01096a031

upstream raw materials:

5-nitro-3-(4-nitro-phenyl)-quinoline

3-methylquinoline

3-phenylquinoline

5-nitro-[3]quinolylamine