3,3-Dimethyl-Z-cyclohexylidenessigsaeure

Base Information

• Chemical Name: 3,3-Dimethyl-Z-cyclohexylidenessigsaeure
• CAS No.: 30346-24-8
• Molecular Formula: C₁₀H₁₆O₂
• Molecular Weight: 168.236
• Mol file: 30346-24-8.mol

Synonyms:

Chemical Property of 3,3-Dimethyl-Z-cyclohexylidenessigsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3-Dimethyl-Z-cyclohexylidenessigsaeure

There total 4 articles about 3,3-Dimethyl-Z-cyclohexylidenessigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-hydroxy-3,3-dimethyl-cyclohexyl)-acetic acid ethyl ester (5629-80-1) → 3,3-Dimethyl-Z-cyclohexylidenessigsaeure (30346-24-8)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. KOH

2: (i) Ac₂O, (ii) aq. KOH, (iii) /BRN= 1098229/, BF₃

3: (hydrolysis)

With potassium hydroxide;

DOI:10.1021/jo00817a012

Reference yield:

3,3-Dimethyl-Z-cyclohexylidenessigsaeuremethylester (30346-23-7) → 3,3-Dimethyl-Z-cyclohexylidenessigsaeure (30346-24-8)

Guidance literature:

(hydrolysis);

DOI:10.1021/jo00817a012

Reference yield:

3,3-Dimethyl-1-hydroxy-cyclohexylessigsaeure (30346-22-6) → 3,3-Dimethyl-Z-cyclohexylidenessigsaeure (30346-24-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) Ac₂O, (ii) aq. KOH, (iii) /BRN= 1098229/, BF₃

2: (hydrolysis)

DOI:10.1021/jo00817a012

upstream raw materials:

3,3-Dimethyl-Z-cyclohexylidenessigsaeuremethylester

3,3-Dimethyl-1-hydroxy-cyclohexylessigsaeure

(1-hydroxy-3,3-dimethyl-cyclohexyl)-acetic acid ethyl ester