WOCl₃(C₁₆H₁₄NO₃)

Base Information

• Chemical Name: WOCl₃(C₁₆H₁₄NO₃)
• CAS No.: 168646-65-9
• Molecular Formula: C₁₆H₁₄Cl₃NO₄W
• Molecular Weight: 574.5
• Mol file: 168646-65-9.mol

Synonyms:

Chemical Property of WOCl₃(C₁₆H₁₄NO₃)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of WOCl₃(C₁₆H₁₄NO₃)

There total 2 articles about WOCl₃(C₁₆H₁₄NO₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tungsten(VI) oxychloride + (E)-ethyl 4-((2-hydroxybenzylidene)amino)benzoate (3246-76-2) → WOCl3(C16H14NO3) (168646-65-9)

Guidance literature:

With diethyl ether; In benzene; boiling soln. of diethyl ether, W-compd. and ligand; hexane addn.; elem. anal.;

Reference yield:

tungsten(VI) oxytrichloroacetylacetonate + (E)-ethyl 4-((2-hydroxybenzylidene)amino)benzoate (3246-76-2) → WOCl3(C16H14NO3) (168646-65-9)

Guidance literature:

In benzene; byproducts: acetylacetone; boiling (1 h); solvent partially destilled off, cooling to room temperature, hexane addn., crystals filtration and washing (hexane), drying (dry Ar flow);

upstream raw materials:

(E)-ethyl 4-((2-hydroxybenzylidene)amino)benzoate

Refernces