MoCl₂(C₆H₄CH₃NCHC₆H₄O)2

Base Information

• Chemical Name: MoCl₂(C₆H₄CH₃NCHC₆H₄O)2
• CAS No.: 36470-60-7
• Molecular Formula: C₂₈H₂₄Cl₂MoN₂O₂
• Molecular Weight: 587.357
• Mol file: 36470-60-7.mol

Synonyms:

Chemical Property of MoCl₂(C₆H₄CH₃NCHC₆H₄O)2

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of MoCl₂(C₆H₄CH₃NCHC₆H₄O)2

There total 2 articles about MoCl₂(C₆H₄CH₃NCHC₆H₄O)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(acetonitrile)tetrachloromolybdenum(IV) (56613-96-8,77210-60-7,15584-93-7,19187-82-7) + N-salicylidene-p-methylaniline (782-76-3) → MoCl2(C6H4CH3NCHC6H4O)2 (36470-60-7,85027-15-2)

Guidance literature:

With triethylamine; In acetonitrile; byproducts: CH3CN; MeCN added to mixt. of Mo complex and ligand, refluxed for 1 h, Et3N added, refluxed for 1 h, under N2; cooled to room temp., filtered off, washed with EtOH, Et2O, dried in vac.;

DOI:10.1039/DT9820002309

Reference yield:

MoCl2(acetylacetonate)2 + N-salicylidene-p-methylaniline (782-76-3) → MoCl2(C6H4CH3NCHC6H4O)2 (36470-60-7,85027-15-2)

Guidance literature:

In acetonitrile; byproducts: acetylacetone; CH3CN added to mixt. of Mo complex and ligand, suspn. refluxed for 0.5 h, under N2; cooled to room temp., filtered off, washed with Et2O, dried in vac.; elem. anal.;

DOI:10.1039/DT9820002309

upstream raw materials:

N-salicylidene-p-methylaniline

bis(acetonitrile)tetrachloromolybdenum(IV)

Refernces