C₁₂H₃₂I₄In₂N₄

Base Information

• Chemical Name: C₁₂H₃₂I₄In₂N₄
• CAS No.: 81985-80-0
• Molecular Formula: C₁₂H₃₂I₄In₂N₄
• Molecular Weight: 969.671
• Mol file: 81985-80-0.mol

Synonyms:

Chemical Property of C₁₂H₃₂I₄In₂N₄

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of C₁₂H₃₂I₄In₂N₄

There total 1 articles about C₁₂H₃₂I₄In₂N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

indium(II) iodide + N,N,N,N,-tetramethylethylenediamine (110-18-9) → C12H32I4In2N4 (81985-80-0) + In2I4((CH3)2NCH2CH2N(CH3)2)2*C6H6

Guidance literature:

With benzene; In benzene; addn. of ligand at -195.8°C under N2 in the minimum amount of solvent, then the cooling bath was removed, and the system was stirred for 20 min after the solvent had completely melted, stirring at room temp. for 2.5 h, then refluxed for 2 h; the solid sepd. on cooling collected and dried, composition In2I4(TMED)2, filtrate concd., viscous liquid settled out on standing, separated, treated with light ligroin (40-60°C) to yield a solid, composition In2I4(TMED)2C6H6; elem. anal.;

DOI:10.1139/v82-101

upstream raw materials:

N,N,N,N,-tetramethylethylenediamine

Refernces