C₄₄H₄₉F₃N₄O₂Si

Base Information

• Chemical Name: C₄₄H₄₉F₃N₄O₂Si
• CAS No.: 958001-69-9
• Molecular Formula: C₄₄H₄₉F₃N₄O₂Si
• Molecular Weight: 750.979
• Mol file: 958001-69-9.mol

Synonyms:

Chemical Property of C₄₄H₄₉F₃N₄O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₄₉F₃N₄O₂Si

There total 7 articles about C₄₄H₄₉F₃N₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5,5-Trimethylcyclohex-2-en-1-one (78-59-1) → C44H49F3N4O2Si (958001-69-9) + C44H49F3N4O2Si

Guidance literature:

Multi-step reaction with 5 steps

1: sodium ethanolate / ethanol / Heating

2: 1H-imidazole / N,N-dimethyl-formamide

3: sodium hydride / tetrahydrofuran / Reflux

4: diisobutylaluminium hydride / toluene / -78 °C

5: ethanol / 60 °C

With 1H-imidazole; sodium ethanolate; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; 3: Wittig-Horner reaction;

DOI:10.1039/c0jm02855j

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → C44H49F3N4O2Si (958001-69-9) + C44H49F3N4O2Si

Guidance literature:

Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide

2: sodium hydride / tetrahydrofuran / Reflux

3: diisobutylaluminium hydride / toluene / -78 °C

4: ethanol / 60 °C

With 1H-imidazole; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; 2: Wittig-Horner reaction;

DOI:10.1039/c0jm02855j

Reference yield:

C28H42N2OSi (1297378-70-1) → C44H49F3N4O2Si (958001-69-9) + C44H49F3N4O2Si

Guidance literature:

Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / toluene / -78 °C

2: ethanol / 60 °C

With diisobutylaluminium hydride; In ethanol; toluene;

DOI:10.1039/c0jm02855j

upstream raw materials:

3,5,5-Trimethylcyclohex-2-en-1-one

C₂₈H₄₂N₂OSi

tert-butyldimethylsilyl chloride

4-(N-ethyl-N-(2-hydroxyethyl)amino)benzaldehyde

Refernces