5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole

Base Information

• Chemical Name: 5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole
• CAS No.: 63517-77-1
• Molecular Formula: C₁₉H₁₄N₆
• Molecular Weight: 326.36
• Mol file: 63517-77-1.mol

Synonyms:

Chemical Property of 5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole

There total 4 articles about 5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole (63517-77-1)

Guidance literature:

With lead dioxide; xylene;

Reference yield:

4-methyl-2,6-bis-phenylazo-m-phenylenediamine (63517-76-0) → 5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole (63517-77-1)

Guidance literature:

With pyridine; copper(I) sulfate; copper(II) sulfate;

Reference yield:

benzene diazonium chloride (100-34-5) → 5-methyl-2,7-diphenyl-2,7-dihydro-benzo[1,2-d;3,4-d']bistriazole (63517-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: natrium carbonate; aqueous alcohol

2: copper sulfate; aqueous pyridine

With pyridine; copper(I) sulfate; ethanol; sodium carbonate; copper(II) sulfate;

upstream raw materials:

4-methyl-2,6-bis-phenylazo-m-phenylenediamine

benzene diazonium chloride

2,4-diamino-5-methylazobenzene