3-nitro-4-o-tolyl-1,2-dihydro-naphthalene

Base Information

• Chemical Name: 3-nitro-4-o-tolyl-1,2-dihydro-naphthalene
• CAS No.: 108973-37-1
• Molecular Formula: C₁₇H₁₅NO₂
• Molecular Weight: 265.312
• Mol file: 108973-37-1.mol

Synonyms:

Chemical Property of 3-nitro-4-o-tolyl-1,2-dihydro-naphthalene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-nitro-4-o-tolyl-1,2-dihydro-naphthalene

There total 3 articles about 3-nitro-4-o-tolyl-1,2-dihydro-naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2-methylphenyl)-1,2-dihydronaphthalene (80710-76-5) → 3-nitro-4-o-tolyl-1,2-dihydro-naphthalene (108973-37-1)

Guidance literature:

With diethyl ether; sulfuric acid; sodium nitrite; Behandeln des Reaktionsprodukts mit Natriummethylat in Methanol;

Reference yield:

(2-methylphenyl)lithium (6699-93-0) → 3-nitro-4-o-tolyl-1,2-dihydro-naphthalene (108973-37-1)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / Erwaermen des Reaktionsprodukts mit wss. H₂SO₄

2: diethyl ether; aqueous H₂SO₄; aqueous NaNO₂ / Behandeln des Reaktionsprodukts mit Natriummethylat in Methanol

With diethyl ether; sulfuric acid; sodium nitrite;

Reference yield:

3,4-dihydronaphthalene-1(2H)-one (529-34-0) → 3-nitro-4-o-tolyl-1,2-dihydro-naphthalene (108973-37-1)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / Erwaermen des Reaktionsprodukts mit wss. H₂SO₄

2: diethyl ether; aqueous H₂SO₄; aqueous NaNO₂ / Behandeln des Reaktionsprodukts mit Natriummethylat in Methanol

With diethyl ether; sulfuric acid; sodium nitrite;

upstream raw materials:

4-(2-methylphenyl)-1,2-dihydronaphthalene

(2-methylphenyl)lithium

3,4-dihydronaphthalene-1(2H)-one