4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid

Base Information

• Chemical Name: 4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid
• CAS No.: 97157-26-1
• Molecular Formula: C₂₇H₂₉NO₆
• Molecular Weight: 463.53
• Mol file: 97157-26-1.mol

Synonyms:

Chemical Property of 4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid

There total 5 articles about 4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4,5-diethoxy-2-phenyloxoacetyl-phenethyl)-benzamide (96075-71-7) → 4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid (97157-26-1)

Guidance literature:

With potassium hydroxide; i-Amyl alcohol;

Reference yield:

(6,7-diethoxy-3,4-dihydro-isoquinolin-1-yl)-phenyl-methanone (102012-61-3) → 4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid (97157-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous NaOH

2: KOH; isoamyl alcohol

With potassium hydroxide; sodium hydroxide; i-Amyl alcohol;

Reference yield:

benzoyl chloride (98-88-4) → 4,5-diethoxy-2-(2-benzoylamino-ethyl)-benzilic acid (97157-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous NaOH

2: KOH; isoamyl alcohol

With potassium hydroxide; sodium hydroxide; i-Amyl alcohol;

upstream raw materials:

N-(4,5-diethoxy-2-phenyloxoacetyl-phenethyl)-benzamide

(6,7-diethoxy-3,4-dihydro-isoquinolin-1-yl)-phenyl-methanone

benzoyl chloride

2-(3,4-diethoxyphenyl)ethylamine