1-<2,3-Diphenyl-allyl>-tosylhydrazid

Base Information

• Chemical Name: 1-<2,3-Diphenyl-allyl>-tosylhydrazid
• CAS No.: 23533-54-2
• Molecular Formula: C₂₂H₂₂N₂O₂S
• Molecular Weight: 378.495
• Mol file: 23533-54-2.mol

Synonyms:

Chemical Property of 1-<2,3-Diphenyl-allyl>-tosylhydrazid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-<2,3-Diphenyl-allyl>-tosylhydrazid

There total 2 articles about 1-<2,3-Diphenyl-allyl>-tosylhydrazid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-1,2-diphenyl-propene (70671-91-9) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 1-<2,3-Diphenyl-allyl>-tosylhydrazid (23533-54-2)

Guidance literature:

Multistep reaction; (i) NaH, DMSO, (ii) /BRN= 2556940/;

DOI:10.1246/bcsj.44.1885

Reference yield:

→ 1-<2,3-Diphenyl-allyl>-tosylhydrazid (23533-54-2)

Guidance literature:

a) 1,2-Diphenyl-3-brom-propen-(1), p-Toluolsulfonyl-hydrazin;

DOI:10.1016/S0040-4039(01)97684-1

Reference yield:

benzaldehyde (100-52-7) + 1-<2,3-Diphenyl-allyl>-tosylhydrazid (23533-54-2) → C29H26N2O2S (33867-11-7)

Guidance literature:

In ethanol;

DOI:10.1246/bcsj.44.1885

upstream raw materials:

3-bromo-1,2-diphenyl-propene

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

C₂₉H₂₆N₂O₂S