2,2,4-Trimethyl-3-oxo-valeriansaeurebenzylamid

Base Information

• Chemical Name: 2,2,4-Trimethyl-3-oxo-valeriansaeurebenzylamid
• CAS No.: 33471-76-0
• Molecular Formula: C₁₅H₂₁NO₂
• Molecular Weight: 247.337
• Mol file: 33471-76-0.mol

Synonyms:

Chemical Property of 2,2,4-Trimethyl-3-oxo-valeriansaeurebenzylamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,2,4-Trimethyl-3-oxo-valeriansaeurebenzylamid

There total 2 articles about 2,2,4-Trimethyl-3-oxo-valeriansaeurebenzylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-isopropylidene-3,3-dimethyl-oxetan-2-one (3173-79-3) + N-benzyl-dithiocarbamic acid ammonium salt (41270-27-3) → 2,2,4-Trimethyl-3-oxo-valeriansaeurebenzylamid (33471-76-0)

Guidance literature:

With pyridine; sulfuric acid; acetic anhydride; Yield given. Multistep reaction; 1.) 2 h, 2.) 30 min;

DOI:10.1002/ardp.19813140704

Reference yield:

4-isopropylidene-3,3-dimethyl-oxetan-2-one (3173-79-3) + benzylamine (100-46-9) → 2,2,4-Trimethyl-3-oxo-valeriansaeurebenzylamid (33471-76-0)

Guidance literature:

upstream raw materials:

4-isopropylidene-3,3-dimethyl-oxetan-2-one

benzylamine

N-benzyl-dithiocarbamic acid ammonium salt

Refernces