2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl

Base Information

• Chemical Name: 2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl
• CAS No.: 107305-91-9
• Molecular Formula: C₂₈H₂₆O₄
• Molecular Weight: 426.512
• Mol file: 107305-91-9.mol

Synonyms:

Chemical Property of 2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl

There total 4 articles about 2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-di-cyclohex-1-enyl-3,5,3',5'-tetramethoxy-biphenyl (103281-92-1) → 2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl (107305-91-9)

Guidance literature:

With chloranil; xylene;

DOI:10.1002/macp.1959.020310110

Reference yield:

3,5,3',5'-tetramethoxybiphenyl (108840-33-1) → 2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl (107305-91-9)

Guidance literature:

Multi-step reaction with 3 steps

1: phenyl lithium; diethyl ether / anschliessend Behandeln mit Cyclohexanon

2: acetyl chloride

3: tetrachloro-<1,4>benzoquinone; xylene

With diethyl ether; chloranil; phenyllithium; acetyl chloride; xylene;

DOI:10.1002/macp.1959.020310110

Reference yield:

1-iodo-3,5-dimethoxybenzene (25245-27-6) → 2',6',3'',5''-tetramethoxy-[1,1';4',1'';4'',1''']quaterphenyl (107305-91-9)

Guidance literature:

Multi-step reaction with 4 steps

1: copper-powder / 260 °C

2: phenyl lithium; diethyl ether / anschliessend Behandeln mit Cyclohexanon

3: acetyl chloride

4: tetrachloro-<1,4>benzoquinone; xylene

With diethyl ether; chloranil; copper; phenyllithium; acetyl chloride; xylene;

DOI:10.1002/macp.1959.020310110

upstream raw materials:

4,4'-di-cyclohex-1-enyl-3,5,3',5'-tetramethoxy-biphenyl

3,5,3',5'-tetramethoxybiphenyl

1-iodo-3,5-dimethoxybenzene

4,4'-Bis-(1-hydroxy-cyclohexyl)-3,5,3',5'-tetramethoxy-biphenyl