2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide)

Base Information

• Chemical Name: 2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide)
• CAS No.: 107412-53-3
• Molecular Formula: C₁₄H₁₂N₂O₅
• Molecular Weight: 288.26
• Mol file: 107412-53-3.mol

Synonyms:

Chemical Property of 2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide)

There total 3 articles about 2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methyl-3-<5-nitro-2-furyl>-acrylsaeure (35904-07-5,7279-49-4) → 2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide) (107412-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: acetone

With thionyl chloride; acetone;

Reference yield:

3-(furan-2-yl)methacrylic acid (54160-39-3) → 2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide) (107412-53-3)

Guidance literature:

Multi-step reaction with 3 steps

1: nitric acid; acetic acid anhydride / -5 °C

2: thionyl chloride

3: acetone

With thionyl chloride; nitric acid; acetic anhydride; acetone;

Reference yield:

2-methyl-3t-(5-nitro-[2]furyl)-acryloyl chloride (7746-90-9) + m-Hydroxyaniline (591-27-5) → 2-methyl-3t-(5-nitro-[2]furyl)-acrylic acid-(3-hydroxy-anilide) (107412-53-3)

Guidance literature:

With acetone;

upstream raw materials:

2-methyl-3t-(5-nitro-[2]furyl)-acryloyl chloride

m-Hydroxyaniline

2-Methyl-3-<5-nitro-2-furyl>-acrylsaeure

3-(furan-2-yl)methacrylic acid