(-)-O-(2-Carboxy-benzoyl)-α-isofenchol

Base Information

• Chemical Name: (-)-O-(2-Carboxy-benzoyl)-α-isofenchol
• CAS No.: 111329-40-9
• Molecular Formula: C₁₈H₂₂O₄
• Molecular Weight: 302.37
• Mol file: 111329-40-9.mol

Synonyms:

Chemical Property of (-)-O-(2-Carboxy-benzoyl)-α-isofenchol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (-)-O-(2-Carboxy-benzoyl)-α-isofenchol

There total 8 articles about (-)-O-(2-Carboxy-benzoyl)-α-isofenchol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalic anhydride (85-44-9) → (-)-O-(2-Carboxy-benzoyl)-α-isofenchol (111329-40-9)

Guidance literature:

at 150 ℃; acidic phthalic acid ester of levorotatory isofenchyl alcohol;

Reference yield:

(-)-(1S,4S)-isofenchone (17957-95-8) → phthalic acid mono-((1S)-1.5.5-trimethyl-norbornyl-(2endo)-ester) (111329-40-9)

Guidance literature:

Multi-step reaction with 2 steps

1: nickel / Hydrogenation

With nickel;

Reference yield:

(1S)-1,5,5-trimethyl-norbornane-2exo-ol (95839-58-0) → phthalic acid mono-((1S)-1.5.5-trimethyl-norbornyl-(2endo)-ester) (111329-40-9)

Guidance literature:

Multi-step reaction with 3 steps

1: bi chromate; sulfuric acid

2: nickel / Hydrogenation

With sulfuric acid; dichromate anion; nickel;

upstream raw materials:

(1S)-1,5,5-trimethyl-norbornane-2exo-ol

phthalic anhydride

(1S)-1,5,5-trimethyl-norbornane-2endo-ol

(-)-(1S,4S)-isofenchone