optically inactive 1-(3-hydroxy-but-1-en-t-yl)-2,2,6-trimethyl-cyclohexanol

Base Information

• Chemical Name: optically inactive 1-(3-hydroxy-but-1-en-t-yl)-2,2,6-trimethyl-cyclohexanol
• CAS No.: 106950-29-2
• Molecular Formula: C₁₃H₂₄O₂
• Molecular Weight: 212.332
• Mol file: 106950-29-2.mol

Synonyms:

Chemical Property of optically inactive 1-(3-hydroxy-but-1-en-t-yl)-2,2,6-trimethyl-cyclohexanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of optically inactive 1-(3-hydroxy-but-1-en-t-yl)-2,2,6-trimethyl-cyclohexanol

There total 6 articles about optically inactive 1-(3-hydroxy-but-1-en-t-yl)-2,2,6-trimethyl-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-hydroxy-but-1-ynyl)-2,2,6-trimethyl-cyclohexanol (41641-09-2) → optically inactive 1-(3-hydroxy-but-1-en-c-yl)-2,2,6-trimethyl-cyclohexanol (106950-29-2)

Guidance literature:

With palladium on activated charcoal; with quinoline deactivated palladium; ethyl acetate;

Reference yield:

1-(3-hydroxy-but-1-ynyl)-2,2,6-trimethyl-cyclohexanol (41641-09-2) → optically inactive 1-(3-hydroxy-but-1-en-t-yl)-2,2,6-trimethyl-cyclohexanol (106950-29-2)

Guidance literature:

With methanol; ammonia; sodium; weiteres Reagens: Aether;

Reference yield:

2,2,6-trimethylcyclohexan-1-one (2408-37-9) → optically inactive 1-(3-hydroxy-but-1-en-c-yl)-2,2,6-trimethyl-cyclohexanol (106950-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: ethyl magnesium bromide

2: with quinoline deactivated palladium/charcoal; ethyl acetate

With palladium on activated charcoal; with quinoline deactivated palladium; ethylmagnesium bromide; ethyl acetate;

upstream raw materials:

1-(3-hydroxy-but-1-ynyl)-2,2,6-trimethyl-cyclohexanol

2,2,6-trimethylcyclohexan-1-one

1-ethynyl-2,2,6-trimethyl-1-cyclohexanol