MoF(C₂₆H₂₄P₂)(C₇H₇)⁽¹⁺⁾*PF₆^(1-) = [MoF(C₂₆H₂₄P₂)(C₇H₇)]PF₆

Base Information

• Chemical Name: MoF(C₂₆H₂₄P₂)(C₇H₇)⁽¹⁺⁾*PF₆^(1-) = [MoF(C₂₆H₂₄P₂)(C₇H₇)]PF₆
• CAS No.: 259530-29-5
• Molecular Formula: C₃₃H₃₁FMoP₂*F₆P
• Molecular Weight: 749.459
• Mol file: 259530-29-5.mol

Synonyms:

Chemical Property of MoF(C₂₆H₂₄P₂)(C₇H₇)⁽¹⁺⁾*PF₆^(1-) = [MoF(C₂₆H₂₄P₂)(C₇H₇)]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of MoF(C₂₆H₂₄P₂)(C₇H₇)⁽¹⁺⁾*PF₆^(1-) = [MoF(C₂₆H₂₄P₂)(C₇H₇)]PF₆

There total 1 articles about MoF(C₂₆H₂₄P₂)(C₇H₇)⁽¹⁺⁾*PF₆^(1-) = [MoF(C₂₆H₂₄P₂)(C₇H₇)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

(acetone){1,2-bis(diphenylphosphino)ethane}(η-cycloheptatrienyl)molybdenum(1+) hexafluorophosphate + lithium fluoride (7789-24-4) → MoF(C26H24P2)(C7H7)(1+)*PF6(1-) = [MoF(C26H24P2)(C7H7)]PF6 (259530-29-5)

Guidance literature:

In acetone; (N2); reflux (1 h); redn. of volume, pptn. on addn. of Et2O, taken up in THF, filtration, repptn. on addn. of Et2O, dissoln. (acetone), pptn. on slow addn. of Et2O;elem. anal.;

DOI:10.1039/a907205e

upstream raw materials:

lithium fluoride

Refernces