N-p-nitrobenzyl-N-isopropylhydroxylamine

Base Information

• Chemical Name: N-p-nitrobenzyl-N-isopropylhydroxylamine
• CAS No.: 191991-35-2
• Molecular Formula: C₁₀H₁₄N₂O₃
• Molecular Weight: 210.233
• Mol file: 191991-35-2.mol

Synonyms:

Chemical Property of N-p-nitrobenzyl-N-isopropylhydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-p-nitrobenzyl-N-isopropylhydroxylamine

There total 1 articles about N-p-nitrobenzyl-N-isopropylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrobenzaldehdye (555-16-8) + N-isopropylhydroxyamine (5080-22-8) → N-p-nitrobenzyl-N-isopropylhydroxylamine (191991-35-2)

Guidance literature:

With sodium tetrahydroborate; Multistep reaction; 1) EtOH, 50-60 deg C, 5 h, 2) EtOH, 50 deg C, 5 h; 20 deg C, 24 h;

DOI:10.1039/a604719j

Reference yield:

acetic anhydride (108-24-7) + N-p-nitrobenzyl-N-isopropylhydroxylamine (191991-35-2) → O-acetyl-N-p-nitrobenzyl-N-isopropylhydroxylamine

Guidance literature:

In dichloromethane; at 0 ℃; for 1h;

DOI:10.1039/a604719j

upstream raw materials:

4-nitrobenzaldehdye

N-isopropylhydroxyamine

Refernces