6-(acetylaminocarbonyl)-3,3-diacetoxy-2,4-di(4-tolyl)-1,2,4,5-tetrazaborine

Base Information

• Chemical Name: 6-(acetylaminocarbonyl)-3,3-diacetoxy-2,4-di(4-tolyl)-1,2,4,5-tetrazaborine
• CAS No.: 137808-23-2
• Molecular Formula: C₂₂H₂₄BN₅O₆
• Molecular Weight: 465.273
• Mol file: 137808-23-2.mol

Synonyms:

Chemical Property of 6-(acetylaminocarbonyl)-3,3-diacetoxy-2,4-di(4-tolyl)-1,2,4,5-tetrazaborine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-(acetylaminocarbonyl)-3,3-diacetoxy-2,4-di(4-tolyl)-1,2,4,5-tetrazaborine

There total 1 articles about 6-(acetylaminocarbonyl)-3,3-diacetoxy-2,4-di(4-tolyl)-1,2,4,5-tetrazaborine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

boric acid (11113-50-1,14635-83-7) + 1,5?bis(4?methylphenyl)?3?cyanoformazan (7014-14-4) → 2,2,7,7-tetraacetoxy-3,6-di(4-tolyl)-1-oxa-3,4,5,6,8-pentaza-2,7-dibora-1,2,7,8-tetrahydronaphthalene (137779-56-7) + 6-(acetylaminocarbonyl)-3,3-diacetoxy-2,4-di(4-tolyl)-1,2,4,5-tetrazaborine (137808-23-2)

Guidance literature:

With acetic anhydride; In acetic acid; boric acid in acetic anhydride and glacial acetic acid is heated at 70-80°C until a clear soln. is obtained; to the soln. is added a soln. of cyanoformazan in acetic anhydride and acetic acid, mixt. is maintained for 11 h at 90-95°C; the mixt. is poured over ice, let stand overnight, ppt. is filtered off, washed with ether, dried in the air, TLC (benzene-octane);

upstream raw materials:

boric acid

1,5?bis(4?methylphenyl)?3?cyanoformazan