(E)-β-(dimethylamino)-2,3,4,5,6-pentafluorostyrene

Base Information

• Chemical Name: (E)-β-(dimethylamino)-2,3,4,5,6-pentafluorostyrene
• CAS No.: 103067-97-6
• Molecular Formula: C₁₀H₈F₅N
• Molecular Weight: 237.172
• Mol file: 103067-97-6.mol

Synonyms:

Chemical Property of (E)-β-(dimethylamino)-2,3,4,5,6-pentafluorostyrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-β-(dimethylamino)-2,3,4,5,6-pentafluorostyrene

There total 2 articles about (E)-β-(dimethylamino)-2,3,4,5,6-pentafluorostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4,5,6-pentafluorophenylacetic acid (653-21-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → (E)-β-(dimethylamino)-2,3,4,5,6-pentafluorostyrene (103067-97-6)

Guidance literature:

With trichlorophosphate; Multistep reaction; 1.) 10 min, 2.) 70 deg C, 2 h;

DOI:10.1021/jo00366a045

Reference yield:

2,3,4,5,6-pentafluorophenylacetic acid (653-21-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → (E)-β-(dimethylamino)-2,3,4,5,6-pentafluorostyrene (103067-97-6) + 2-(pentafluorophenyl)-3-(dimethylamino)acrolein (103025-40-7)

Guidance literature:

With trichlorophosphate; multistep reaction; product yield/distribution; var. reaction time; other substituted acetic acids;

DOI:10.1021/jo00366a045

upstream raw materials:

2,3,4,5,6-pentafluorophenylacetic acid

N,N-dimethyl-formamide

Refernces