dichloro-[1-methyl-2-(phenylazo)imidazole]zinc(II) monohydrate

Base Information

• Chemical Name: dichloro-[1-methyl-2-(phenylazo)imidazole]zinc(II) monohydrate
• CAS No.: 630391-68-3
• Molecular Formula: C₁₀H₁₂Cl₂N₄OZn
• Molecular Weight: 340.527
• Mol file: 630391-68-3.mol

Synonyms:

Chemical Property of dichloro-[1-methyl-2-(phenylazo)imidazole]zinc(II) monohydrate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of dichloro-[1-methyl-2-(phenylazo)imidazole]zinc(II) monohydrate

There total 1 articles about dichloro-[1-methyl-2-(phenylazo)imidazole]zinc(II) monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

zinc(II) chloride monohydrate + 1-methyl-2-(phenylazo)imidazole (72908-92-0,93937-86-1) → dichloro-[1-methyl-2-(phenylazo)imidazole]zinc(II) monohydrate (630391-68-3)

Guidance literature:

In methanol; ligand in CH3OH added dropwise to ZnCl2 in CH3OH at room temp. for 3 h; concd.(air), crystd.(refrigerator, 5°C), filtered, washed (water,cold CH3OH), recrystd.(CH3OH-H2O 1:1 v/v), dried (CaCl2), elem. anal.;

DOI:10.1016/S0277-5387(03)00111-6

upstream raw materials:

1-methyl-2-(phenylazo)imidazole

Refernces