Diazene, 1,1'-(1,4-phenylene)bis[2-[4-(phenylazo)phenyl]-(9CI)

Base Information

• Chemical Name: Diazene, 1,1'-(1,4-phenylene)bis[2-[4-(phenylazo)phenyl]-(9CI)
• CAS No.: 96374-99-1
• Molecular Formula: C₃₀H₂₂N₈
• Molecular Weight: 494.558
• DSSTox Substance ID: DTXSID701038700
• Mol file: 96374-99-1.mol

Synonyms:DTXSID701038700;AKOS004904990;Diazene, 1,1'-(1,4-phenylene)bis[2-[4-(phenylazo)phenyl]- (9CI);96374-99-1

Chemical Property of Diazene, 1,1'-(1,4-phenylene)bis[2-[4-(phenylazo)phenyl]-(9CI)

Chemical Property:

• XLogP3: 9.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 8
• Exact Mass: 494.19674274
• Heavy Atom Count: 38
• Complexity: 708

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N=NC2=CC=C(C=C2)N=NC3=CC=C(C=C3)N=NC4=CC=C(C=C4)N=NC5=CC=CC=C5

Technology Process of Diazene, 1,1'-(1,4-phenylene)bis[2-[4-(phenylazo)phenyl]-(9CI)

There total 7 articles about Diazene, 1,1'-(1,4-phenylene)bis[2-[4-(phenylazo)phenyl]-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-benzoquinone dioxime (105-11-3,6133-83-1,6421-98-3) → 1,4-bis-[4-(phenyl-trans-azo)-phenyl-trans-azo]-benzene (96374-99-1)

Guidance literature:

Multi-step reaction with 2 steps

1: K₃fe(CN)6; aqueous alkaline solution

2: acetic acid

With alkaline solution; acetic acid; potassium hexacyanoferrate(III);

DOI:10.1002/hlca.19380210195

Reference yield:

p-dinitrosobenzene (105-12-4,9003-34-3) → 1,4-bis-[4-(phenyl-trans-azo)-phenyl-trans-azo]-benzene (96374-99-1)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol; acetic acid

2: ethanolic KOH-solution

3: acetic acid

With potassium hydroxide; ethanol; acetic acid;

DOI:10.1002/hlca.19380210195

Reference yield:

1,4-bis-(4-amino-phenylazo)-benzene (21371-46-0) + Nitrosobenzene (586-96-9) → 1,4-bis-[4-(phenyl-trans-azo)-phenyl-trans-azo]-benzene (96374-99-1)

Guidance literature:

With acetic acid;

DOI:10.1002/hlca.194102401130 DOI:10.1002/hlca.19380210195

upstream raw materials:

p-dinitrosobenzene

aniline yellow

1-(4-amino-phenylazo)-4-(4-amino-phenyl-NNO-azoxy)-benzene

Nitrosobenzene