Technology Process of Benzenesulfonic acid, 4-hexyl-, potassium salt
There total 1 articles about Benzenesulfonic acid, 4-hexyl-, potassium salt which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: POCl3 / a.) 170 deg C, 1 h, b.) dichloroethane, 60 deg C, 30 min
2: 88 percent / H2SO4 conc., Zn powder / H2O / 2 h / 100 °C
3: 84 percent / K2CO3 / acetone / 2 h / Heating
4: SOCl2, N,N-dimethylformamide / 1 h / Ambient temperature
5: AlCl3 / 1,2-dichloro-ethane / 1 h / Ambient temperature
6: 88 percent / piperidine / benzene / 1 h / Heating
7: 56 percent / K2CO3 / acetone / 70 °C
With
piperidine; aluminium trichloride; thionyl chloride; sulfuric acid; potassium carbonate; N,N-dimethyl-formamide; zinc; trichlorophosphate;
In
water; 1,2-dichloro-ethane; acetone; benzene;
DOI:10.1246/bcsj.65.649
- Guidance literature:
-
Multi-step reaction with 4 steps
1: POCl3 / a.) 170 deg C, 1 h, b.) dichloroethane, 60 deg C, 30 min
2: 88 percent / H2SO4 conc., Zn powder / H2O / 2 h / 100 °C
3: 84 percent / K2CO3 / acetone / 2 h / Heating
4: SOCl2, N,N-dimethylformamide / 1 h / Ambient temperature
With
thionyl chloride; sulfuric acid; potassium carbonate; N,N-dimethyl-formamide; zinc; trichlorophosphate;
In
water; acetone;
DOI:10.1246/bcsj.65.649
