VO⁽²⁺⁾*(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NCl*SO₄^(2-)=VO(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NClSO₄

Base Information

• Chemical Name: VO⁽²⁺⁾*(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NCl*SO₄^(2-)=VO(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NClSO₄
• CAS No.: 107632-46-2
• Molecular Formula: C₂₀H₂₂ClN₃O*OV*O₄S
• Molecular Weight: 518.872
• Mol file: 107632-46-2.mol

Synonyms:

Chemical Property of VO⁽²⁺⁾*(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NCl*SO₄^(2-)=VO(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NClSO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of VO⁽²⁺⁾*(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NCl*SO₄^(2-)=VO(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NClSO₄

There total 1 articles about VO⁽²⁺⁾*(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NCl*SO₄^(2-)=VO(C₂H₅)2NCH₂C₆H₃OHNHC₉H₅NClSO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxovanadium(IV) sulfate + amodiaquine hydrochloride (69-44-3,118490-14-5) → VO(2+)*(C2H5)2NCH2C6H3OHNHC9H5NCl*SO4(2-)=VO(C2H5)2NCH2C6H3OHNHC9H5NClSO4 (107632-46-2,117198-69-3)

Guidance literature:

In water; an aq. soln. of VOSO4 was mixed with an aq. soln. of org. compd. in 1:1stoich. ratio; the react. mixt. was refluxed for 0.5 - 1 h on a water bath;; the volume of the react. mixt. was reduced to about one third, sepn. ofthe product on cooling; it was filtered and washed with ice cold water and dried over P4O10 in vacuo; purifn. by recrystn. from ethyl alcohol; elem. anal.;;

DOI:10.1016/S0020-1693(00)83277-6

upstream raw materials:

amodiaquine hydrochloride