2-tert-butylthiomethyl-N-tert-butoxycarbonylaniline

Base Information

• Chemical Name: 2-tert-butylthiomethyl-N-tert-butoxycarbonylaniline
• CAS No.: 164226-16-8
• Molecular Formula: C₁₆H₂₅NO₂S
• Molecular Weight: 295.446
• Mol file: 164226-16-8.mol

Synonyms:

Chemical Property of 2-tert-butylthiomethyl-N-tert-butoxycarbonylaniline

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-tert-butylthiomethyl-N-tert-butoxycarbonylaniline

There total 1 articles about 2-tert-butylthiomethyl-N-tert-butoxycarbonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl disulfide (110-06-5) + N-(tert-butoxycarbonyl)-o-toluidine (74965-31-4) → 2-tert-butylthiomethyl-N-tert-butoxycarbonylaniline (164226-16-8)

Guidance literature:

With sec.-butyllithium; Yield given. Multistep reaction; 1.) cyclohexane, THF, -40 deg C, 20 min, 2.) cyclohexane, THF, -40 deg C, 30 min;

DOI:10.1139/v95-045

upstream raw materials:

di-tert-butyl disulfide

N-(tert-butoxycarbonyl)-o-toluidine

Refernces