Pyridine, 3-methyl-, hydrochloride

Base Information

• Chemical Name: Pyridine, 3-methyl-, hydrochloride
• CAS No.: 14401-92-4
• Molecular Formula: C6H7N.ClH
• Molecular Weight: 129.589
• DSSTox Substance ID: DTXSID20480082
• Mol file: 14401-92-4.mol

Synonyms:14401-92-4;Pyridine, 3-methyl-, hydrochloride;3-methylpyridine hydrochloride;3-methylpyridine;hydrochloride;Pyridine, 3-methyl-, hydrochloride (1:1);DTXSID20480082

Chemical Property of Pyridine, 3-methyl-, hydrochloride

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 129.0345270
• Heavy Atom Count: 8
• Complexity: 52.1

Purity/Quality:

>95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CN=CC=C1.Cl

Technology Process of Pyridine, 3-methyl-, hydrochloride

There total 1 articles about Pyridine, 3-methyl-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Methylpyridine (108-99-6) + 2,2-Dimethyl-1,3-propanediol (126-30-7) → 5,5,5',5'-tetramethyl-2,2'-oxy-bis-[1,3,2]dioxaphosphinane 2,2'-disulfide (4090-51-1) + 3-methylpyridinium chloride (14401-92-4)

Guidance literature:

With trichlorothiophosphine; water; at 50 - 60 ℃; Product distribution / selectivity;

Reference yield:

3-methylpyridinium chloride (14401-92-4) + 4-methoxy-aniline (104-94-9) → 2-(4-methoxylphenyl)-5-methylpyridine (25363-55-7) + 2-(4-methoxyphenyl)-3-methyl-pyridine (25363-50-2) + 4-(4-methoxyphenyl)-3-methylpyridine (76160-92-4)

Guidance literature:

4-methoxy-aniline; With tetrafluoroboric acid; sodium nitrite; In water; at 0 ℃; Inert atmosphere;

3-methylpyridinium chloride; With tris(bipyridine)ruthenium(II) dichloride hexahydrate; In water; at 25 ℃; for 80h; Catalytic behavior; Irradiation; Inert atmosphere;

DOI:10.1002/chem.201304120

upstream raw materials:

3-Methylpyridine

2,2-Dimethyl-1,3-propanediol

Downstream raw materials:

2-(4-methoxylphenyl)-5-methylpyridine

2-(4-methoxyphenyl)-3-methyl-pyridine

4-(4-methoxyphenyl)-3-methylpyridine

Refernces