Trit-Glu(OtBu)-OH_.Et₂NH

Base Information

• Chemical Name: Trit-Glu(OtBu)-OH_.Et₂NH
• CAS No.: 86967-52-4
• Molecular Formula: C₄H₁₁N*C₂₈H₃₁NO₄
• Molecular Weight: 518.696
• Mol file: 86967-52-4.mol

Synonyms:

Chemical Property of Trit-Glu(OtBu)-OH_.Et₂NH

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Trit-Glu(OtBu)-OH_.Et₂NH

There total 1 articles about Trit-Glu(OtBu)-OH_.Et₂NH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

γ-tert butyl ester of glutamic acid (2419-56-9,45125-00-6) + trityl chloride (76-83-5) + diethylamine (109-89-7) → Trit-Glu(OtBu)-OH.Et2NH (86967-52-4)

Guidance literature:

With bis-(trimethylsilyl)acetamide; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, 2.) O deg C, 2h, room temp., 6h, 3.) Et₂O;

DOI:10.1007/BF00580560

upstream raw materials:

γ-tert butyl ester of glutamic acid

trityl chloride

diethylamine

Refernces