Benzenemethanamine, N-hydroxy-a-phenyl-

Base Information

• Chemical Name: Benzenemethanamine, N-hydroxy-a-phenyl-
• CAS No.: 1485-71-8
• Molecular Formula: C13H13NO
• Molecular Weight: 199.252
• Mol file: 1485-71-8.mol

Synonyms:

Chemical Property of Benzenemethanamine, N-hydroxy-a-phenyl-

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, N-hydroxy-a-phenyl-

There total 20 articles about Benzenemethanamine, N-hydroxy-a-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Benzophenone oxime (574-66-3) → benzophenone oxime (1485-71-8)

Guidance literature:

With hydrogenchloride; sodium cyanoborohydride; In methanol; at 20 ℃; for 4h; pH=3;

DOI:10.1021/ol0711568

Reference yield: 53.0%

C15H12N2O (300843-74-7) → benzophenone oxime (1485-71-8)

Guidance literature:

With hydroxylamine hydrochloride; In methanol; at 60 ℃; for 24h;

DOI:10.1039/b505324b

Reference yield: 20.0%

2-benzhydryl-3-(4-methoxyphenyl)-1,2-oxaziridine (107836-62-4,107836-63-5,1070912-86-5) → benzophenone oxime (1485-71-8)

Guidance literature:

2-benzhydryl-3-(4-methoxyphenyl)-1,2-oxaziridine; With hydroxylamine hydrochloride; In methanol; at 20 ℃; for 16h;

With sodium hydroxide; In methanol; water; pH=13;

upstream raw materials:

Bromodiphenylmethane

acetone oxime

Benzophenone oxime

benzophenone O-acetyl oxime

Downstream raw materials:

N-benzhydryl-O-benzoyl-hydroxylamine

N-benzhydryl-N-hydroxy-benzamide

N-<<(4S,5S)-2,2,5-trimethyl-1,3-dioxolan-4-yl>methylene>benzhydrylamine N-oxide

N-<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylene>benzhydrylamine N-oxide

Refernces

• 1、 Ciotonea, Carmen,Hammi, Nisrine,Dhainaut, Jérémy,Marinova, Maya,Ungureanu, Adrian,El Kadib, Abdelkrim,Michon, Christophe,Royer, Sébastien. "Phyllosilicate-derived Nickel-cobalt Bimetallic Nanoparticles for the Catalytic Hydrogenation of Imines, Oximes and N-heteroarenes". . p. 4652 - 4663. Retrieved 2020/08/19.
• 2、 Sivappa, Rasapalli,Hernandez, Nora M.,He, Yong,Lovely, Carl J.. "Studies toward the total synthesis of axinellamine and massadine". . p. 3861 - 3864. Retrieved 2008/02/11.