1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane

Base Information

• Chemical Name: 1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane
• CAS No.: 120233-13-8
• Molecular Formula: C₄₈H₆₀N₁₂O₁₆
• Molecular Weight: 1061.08
• Mol file: 120233-13-8.mol

Synonyms:

Chemical Property of 1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane

There total 3 articles about 1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,8,15,22-tetraaza-cyclooctacosane-2,9,16,23-tetraone (5834-63-9) → 1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane (120233-13-8)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄; THF

2: aqueous NaHCO₃; ethanol

With tetrahydrofuran; lithium aluminium tetrahydride; ethanol; sodium hydrogencarbonate;

Reference yield:

1,8,15,22-tetraaza-cyclooctacosane-2,7,16,21-tetraone (4238-35-1) → 1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane (120233-13-8)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄; THF

2: aqueous NaHCO₃; ethanol

With tetrahydrofuran; lithium aluminium tetrahydride; ethanol; sodium hydrogencarbonate;

Reference yield:

1,8,15,22-tetraazacyclooctacontane (297-28-9) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → 1,8,15,22-tetrakis-(2,4-dinitro-phenyl)-1,8,15,22-tetraaza-cyclooctacosane (120233-13-8)

Guidance literature:

With ethanol; sodium hydrogencarbonate;

upstream raw materials:

1,8,15,22-tetraazacyclooctacontane

2,4-Dinitrofluorobenzene

1,8,15,22-tetraaza-cyclooctacosane-2,9,16,23-tetraone

1,8,15,22-tetraaza-cyclooctacosane-2,7,16,21-tetraone