2-[3-(2-furyl)propyl]furan

Base Information

• Chemical Name: 2-[3-(2-furyl)propyl]furan
• CAS No.: 5447-79-0
• Molecular Formula: C11H12 O2
• Molecular Weight: 176.21
• Hs Code.: 2932190090
• Mol file: 5447-79-0.mol

Synonyms:Furan,2,2'-trimethylenedi- (6CI,8CI); NSC 17526

Chemical Property of 2-[3-(2-furyl)propyl]furan

Chemical Property:

• Boiling Point: 230.6°Cat760mmHg
• Flash Point: 89°C
• PSA: 26.28000
• Density: 1.067g/cm³
• LogP: 3.04790

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[3-(2-furyl)propyl]furan

There total 4 articles about 2-[3-(2-furyl)propyl]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

furan (110-00-9) + 1,3-dibromo-propane (109-64-8) → 1,3-di(furan-2-yl)propane (5447-79-0)

Guidance literature:

furan; With n-butyllithium;

1,3-dibromo-propane;

DOI:10.1016/j.polymer.2014.06.041

Reference yield: 38.0%

2-lithiofuran (2786-02-9) + 1,3-Diiodopropane (627-31-6) → 1,3-di(furan-2-yl)propane (5447-79-0)

Guidance literature:

DOI:10.1021/jo961635c

Reference yield:

furan (110-00-9) + 1,3-dibromo-propane (109-64-8) → furnish 2-(3-bromopropyl)furan (92513-83-2) + 1,3-di(furan-2-yl)propane (5447-79-0)

Guidance literature:

furan; With n-butyllithium; In tetrahydrofuran; hexane; at 60 ℃; for 1h; Inert atmosphere; Cooling with acetone-dry ice;

1,3-dibromo-propane; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere; Cooling with acetone-dry ice;

DOI:10.1002/chem.201101015

upstream raw materials:

2-lithiofuran

1,3-Diiodopropane

furan

1,3-dibromo-propane

Refernces

• 1、 Klumpp, Douglas A.,Gilbert, Thomas M.,Trahanovsky, Walter S.. "Intramolecular Reactions of Tethered Furan-Based Bis(p-quinodimethanes)". . p. 5559 - 5568. Retrieved 2016.
• 2、 Lautens, Mark,Fillion, Eric. "An Expedient Route for the Stereoselective Construction of Bridged Polyheterocyclic Ring Systems Using the Tandem "Pincer" Diels-Alder Reaction". . p. 4418 - 4427. Retrieved 2007/10/03.