NITROACETONE

Base Information

• Chemical Name: NITROACETONE
• CAS No.: 10230-68-9
• Molecular Formula: C3H5NO3
• Molecular Weight: 103.078
• Mol file: 10230-68-9.mol

Synonyms:2-Propanone,nitro- (6CI,7CI);1-Nitro-2-propanone;Nitroacetone;

Chemical Property of NITROACETONE

Chemical Property:

• Vapor Pressure: 1.36mmHg at 25°C
• Melting Point: 50.3°C
• Refractive Index: 1.414
• Boiling Point: 172.1 °C at 760 mmHg
• Flash Point: 73.8 °C
• PSA: 62.89000
• Density: 1.171 g/cm³
• LogP: 0.37530

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Propanone,1-nitro- 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1-?Nitropropan-?2-?on is a reactant used in the synthesis of deoxyaminosugars.

Technology Process of NITROACETONE

There total 2 articles about NITROACETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl ether (60-29-7,927820-24-4) + 1-(4-Methoxyphenyl)-2-nitro-1-buten-3-one (88818-49-9) + ammonia (7664-41-7) → 1-nitro-2-propanone (10230-68-9) + 4-methoxy-benzaldehyde (123-11-5)

Guidance literature:

Reference yield:

→ 1-nitro-2-propanone (10230-68-9) + 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-5-nitropyridine-3-carboxylic acid

Guidance literature:

Reference yield: 91.0%

1-nitro-2-propanone (10230-68-9) + C12H12O3 (1201664-50-7) → C15H17NO6

Guidance literature:

C₁₂H₁₂O₃; With 1-(((1R,4aS,10aR)-7-isopropyl-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthren-1-yl)methyl)-3-((1S,2S)-2-(pyrrolidin-1-yl)cyclohexyl)thiourea; In toluene; at -15 ℃; for 36h;

1-nitro-2-propanone; In toluene;

DOI:10.1016/j.cclet.2013.12.024

upstream raw materials:

diethyl ether

1-(4-Methoxyphenyl)-2-nitro-1-buten-3-one

ammonia

Downstream raw materials:

1-nitro-1-(3-nitro-phenylhydrazono)-acetone

1-nitro-1-(2,4,6-tribromo-phenylhydrazono)-acetone

1-(4-Methoxyphenyl)-2-nitro-1-buten-3-one

3-nitro-4-(4-nitro-phenyl)-but-3-en-2-one

Refernces