Technology Process of 1H-Imidazole-5-carboxaldehyde, 4-amino-1-(phenylmethyl)-, oxime
There total 4 articles about 1H-Imidazole-5-carboxaldehyde, 4-amino-1-(phenylmethyl)-, oxime which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
for 4h;
under 2.8 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 78 percent / AgClO4 / toluene; H2O / 2.5 h / Heating
2: 30 percent / hydroxylamine hydrochloride, HCO2Na, formic acid / 2 h / Heating
3: 100 percent / H2 / 10percent Pd/C / methanol / 4 h / 2.8 Torr
With
formic acid; hydroxylamine hydrochloride; hydrogen; sodium formate; silver perchlorate;
palladium on activated charcoal;
In
methanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80.5 percent / t-BuOK / tetrahydrofuran; dimethylformamide / 0.33 h / -70 °C
2: 78 percent / AgClO4 / toluene; H2O / 2.5 h / Heating
3: 30 percent / hydroxylamine hydrochloride, HCO2Na, formic acid / 2 h / Heating
4: 100 percent / H2 / 10percent Pd/C / methanol / 4 h / 2.8 Torr
With
formic acid; hydroxylamine hydrochloride; potassium tert-butylate; hydrogen; sodium formate; silver perchlorate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;
