Sn(C₆H₅)3(NCSe)((CH₂)4SO)

Base Information

• Chemical Name: Sn(C₆H₅)3(NCSe)((CH₂)4SO)
• CAS No.: 79268-59-0
• Molecular Formula: C₂₃H₂₃NOSSeSn
• Molecular Weight: 559.178
• Mol file: 79268-59-0.mol

Synonyms:

Chemical Property of Sn(C₆H₅)3(NCSe)((CH₂)4SO)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Sn(C₆H₅)3(NCSe)((CH₂)4SO)

There total 1 articles about Sn(C₆H₅)3(NCSe)((CH₂)4SO) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-oxothiolane (1600-44-8) + potassium selenocyanate (3425-46-5) + triphenyltin chloride (639-58-7) → Sn(C6H5)3(NCSe)((CH2)4SO) (79268-59-0)

Guidance literature:

In acetone; byproducts: KCl; N2 atmosphere; a mixt. of Ph3SnCl and KSeCN in dry acetone was stirred in the presence of K2CO3 at room temp. for several hours; filtration (sepn. of KCl); addn. of an excess of ligand in acetone; refluxed for 2-3 h;; concn. by distn.; crystn. on cooling (addn. of Et2O or petroleum ether if need be); repeatedly washed; dried under vac.; elem. anal.;;

upstream raw materials:

1-oxothiolane

potassium selenocyanate

triphenyltin chloride

Refernces