C₉₆H₁₄₄N₃₀O₁₇

Base Information

• Chemical Name: C₉₆H₁₄₄N₃₀O₁₇
• CAS No.: 1315576-99-8
• Molecular Formula: C₉₆H₁₄₄N₃₀O₁₇
• Molecular Weight: 1990.39
• Mol file: 1315576-99-8.mol

Synonyms:

Chemical Property of C₉₆H₁₄₄N₃₀O₁₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of C₉₆H₁₄₄N₃₀O₁₇

There total 1 articles about C₉₆H₁₄₄N₃₀O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fmoc-Leu-OH (35661-60-0) + Fmoc-Pro-OH (71989-31-6) + N-Fmoc L-Phe (35661-40-6) + Fmoc-Ser(tBu)-OH (71989-33-8) + Fmoc-D-Phe-OH (86123-10-6) + 3-propionic acid (80028-35-9) + N-2,N-6-bis(9-fluorenylmethyloxycarbonyl)-L-lysine (75932-02-4,78081-87-5) + (2S,4R)-4-tert-butoxy-1-(9H-fluoren-9-ylmethoxycarbonyl)pyrrolidine-2-carboxylic acid (268729-12-0) + (S)-6-[(Diphenyl-p-tolyl-methyl)-amino]-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoic acid + Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine (187618-60-6) + N-α-[(9H-fluoren-9-ylmethoxy)carbonyl]-NG-(2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl)-D-arginine (187618-60-6) → C96H144N30O17 (1315576-99-8)

Guidance literature:

Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; Inert atmosphere; solid phase reaction;

With piperidine; In 1-methyl-pyrrolidin-2-one; Inert atmosphere; solid phase reaction;

Fmoc-Leu-OH; Fmoc-Pro-OH; N-Fmoc L-Phe; Fmoc-Ser(tBu)-OH; Fmoc-D-Phe-OH; 3-propionic acid; N-2,N-6-bis(9-fluorenylmethyloxycarbonyl)-L-lysine; (2S,4R)-4-tert-butoxy-1-(9H-fluoren-9-ylmethoxycarbonyl)pyrrolidine-2-carboxylic acid; (S)-6-[(Diphenyl-p-tolyl-methyl)-amino]-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoic acid; N-α-[(9H-fluoren-9-ylmethoxy)carbonyl]-N^G-(2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl)-D-arginine; Further stages;

DOI:10.1021/ja204422r

upstream raw materials:

Fmoc-Leu-OH

Fmoc-Pro-OH

N-Fmoc L-Phe

Fmoc-Ser(tBu)-OH

Refernces