Technology Process of (Nitrooxy)oxobismuthine
There total 11 articles about (Nitrooxy)oxobismuthine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
nitric acid;
aq. HNO3; formation of the sparingly soluble basic salts; solution of the salts if H(1+)-activity exceeds 0.06;;
DOI:10.1021/ja01146a001
- Guidance literature:
-
With
water;
In
nitric acid;
byproducts: N oxide; preparation of a layer of 165 g remolten Bi (description of method given) and solvation at 60-70°C in 1040 ml 25% HNO3; vigorous reaction, form. of N oxide; filtration and evaporation in porcelain crucibles; addition of 800 ml H2O under stirring;; addition of the mass to hot water and washing the precipitate with H2O; drying with alcohol and heating at 45°C;;
- Guidance literature:
-
In
neat (no solvent);
drying over H2SO4 or in a stream of CO2 or dry air to constant weight;;