2-bromo-N-carbamoyl-3,3-dimethylbutanamide

Base Information

• Chemical Name: 2-bromo-N-carbamoyl-3,3-dimethylbutanamide
• CAS No.: 6632-50-4
• Molecular Formula: C₇H₁₃BrN₂O₂
• Molecular Weight: 237.096
• Mol file: 6632-50-4.mol

Synonyms:Urea,(2-bromo-3,3-dimethylbutyryl)- (8CI); NSC 57697

Chemical Property of 2-bromo-N-carbamoyl-3,3-dimethylbutanamide

Chemical Property:

• Density: 1.441g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-bromo-N-carbamoyl-3,3-dimethylbutanamide

There total 5 articles about 2-bromo-N-carbamoyl-3,3-dimethylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,4-trimethyl-1-pentene (107-39-1) → (2-bromo-3,3-dimethyl-butyryl)-urea (6632-50-4)

Guidance literature:

Multi-step reaction with 5 steps

1: Cr₂O₃-H₂SO₄

2: NaOBr

3: SOCl₂

4: bromine

With chromium(III) oxide; thionyl chloride; sodium hypobromide; sulfuric acid; bromine;

DOI:10.1021/ja01337a055

Reference yield:

4,4-dimethyl-pentan-2-one (590-50-1) → (2-bromo-3,3-dimethyl-butyryl)-urea (6632-50-4)

Guidance literature:

Multi-step reaction with 4 steps

1: NaOBr

2: SOCl₂

3: bromine

With thionyl chloride; sodium hypobromide; bromine;

DOI:10.1021/ja01337a055

Reference yield:

3,3-dimethylbutanoic acid chloride (7065-46-5) → (2-bromo-3,3-dimethyl-butyryl)-urea (6632-50-4)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine

With bromine;

DOI:10.1021/ja01337a055

upstream raw materials:

2-bromo-3,3-dimethylbutanoyl chloride

urea

2,4,4-trimethyl-1-pentene

4,4-dimethyl-pentan-2-one