Technology Process of Hexanal, 2-ethyl-2-[[[2-(phenylmethyl)phenyl]sulfonyl]methyl]-
There total 16 articles about Hexanal, 2-ethyl-2-[[[2-(phenylmethyl)phenyl]sulfonyl]methyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol; dichloromethane;
at 20 ℃;
for 14h;
under 3620.04 Torr;
DOI:10.1021/jm040215+
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 20.5 g / Et3N / various solvent(s) / 24 h / Heating
2: 1.9 g / mCPBA / CH2Cl2 / 64 h / 20 °C
3: H2 / Pd/C / CH2Cl2; methanol / 14 h / 20 °C / 3620.04 Torr
With
hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid;
palladium on activated charcoal;
In
methanol; dichloromethane;
DOI:10.1021/jm040215+
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N / 18 h / 20 °C
2: 20.5 g / Et3N / various solvent(s) / 24 h / Heating
3: 1.9 g / mCPBA / CH2Cl2 / 64 h / 20 °C
4: H2 / Pd/C / CH2Cl2; methanol / 14 h / 20 °C / 3620.04 Torr
With
hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid;
palladium on activated charcoal;
In
methanol; dichloromethane;
DOI:10.1021/jm040215+
