(3-benzyl-2-dimethylamino-[1,3,2]diazaphospholidin-1-yl)-phosphonous acid bis-dimethylamide

Base Information

• Chemical Name: (3-benzyl-2-dimethylamino-[1,3,2]diazaphospholidin-1-yl)-phosphonous acid bis-dimethylamide
• CAS No.: 67696-34-8
• Molecular Formula: C₁₅H₂₉N₅P₂
• Molecular Weight: 341.376
• Mol file: 67696-34-8.mol

Synonyms:

Chemical Property of (3-benzyl-2-dimethylamino-[1,3,2]diazaphospholidin-1-yl)-phosphonous acid bis-dimethylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3-benzyl-2-dimethylamino-[1,3,2]diazaphospholidin-1-yl)-phosphonous acid bis-dimethylamide

There total 2 articles about (3-benzyl-2-dimethylamino-[1,3,2]diazaphospholidin-1-yl)-phosphonous acid bis-dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Hexamethylphosphorous triamide (1608-26-0) + N-benzylethylenediamine (4152-09-4) → (3-benzyl-2-dimethylamino-[1,3,2]diazaphospholidin-1-yl)-phosphonous acid bis-dimethylamide (67696-34-8)

Guidance literature:

at 110 - 150 ℃;

DOI:10.1007/BF00946889

Reference yield:

→ (3-benzyl-2-dimethylamino-[1,3,2]diazaphospholidin-1-yl)-phosphonous acid bis-dimethylamide (67696-34-8)

Guidance literature:

Phosphorigsaeure-tris-(dimethylamid), N-Benzyl-aethylendiamin, 140-150grad, 1h;

upstream raw materials:

Hexamethylphosphorous triamide

N-benzylethylenediamine