Technology Process of Carbamic acid, [1-methyl-2-(1-phenylhydrazino)ethyl]-, methyl ester
There total 4 articles about Carbamic acid, [1-methyl-2-(1-phenylhydrazino)ethyl]-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid; zinc;
In
water;
for 1h;
Ambient temperature;
DOI:10.1021/jm960372b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / oxalyl chloride, DMSO, Et3N / CH2Cl2 / 1 h / -78 - 20 °C
2: 45 percent / NaBH3CN / methanol / 16 h / Ambient temperature; pH 5-6
3: 97 percent / concd HCl, NaNO2 / H2O / 1 h / 0 °C
4: Zn (dust), acetic acid / H2O / 1 h / Ambient temperature
With
hydrogenchloride; oxalyl dichloride; sodium cyanoborohydride; acetic acid; dimethyl sulfoxide; triethylamine; zinc; sodium nitrite;
In
methanol; dichloromethane; water;
DOI:10.1021/jm960372b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 45 percent / NaBH3CN / methanol / 16 h / Ambient temperature; pH 5-6
2: 97 percent / concd HCl, NaNO2 / H2O / 1 h / 0 °C
3: Zn (dust), acetic acid / H2O / 1 h / Ambient temperature
With
hydrogenchloride; sodium cyanoborohydride; acetic acid; zinc; sodium nitrite;
In
methanol; water;
DOI:10.1021/jm960372b