Technology Process of Benzene, 1,3,5-tris(2-bromoethyl)-
There total 6 articles about Benzene, 1,3,5-tris(2-bromoethyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / ethanol; water / 100 °C / Sealed tube
2: sulfuric acid / methanol / 18 h / 72 °C / Sealed tube
3: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
4: hydrogen bromide / water / 5 h / 125 °C / Sealed tube
With
lithium aluminium tetrahydride; sulfuric acid; hydrogen bromide; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/acs.jmedchem.1c01482
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydrogencarbonate / tetrahydrofuran; water / 3 h / 20 °C
2: potassium hydroxide / ethanol; water / 100 °C / Sealed tube
3: sulfuric acid / methanol / 18 h / 72 °C / Sealed tube
4: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
5: hydrogen bromide / water / 5 h / 125 °C / Sealed tube
With
lithium aluminium tetrahydride; sulfuric acid; hydrogen bromide; sodium hydrogencarbonate; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/acs.jmedchem.1c01482