2-cyanoethyl acetate

Base Information

• Chemical Name: 2-cyanoethyl acetate
• CAS No.: 5325-93-9
• Molecular Formula: C5H7NO2
• Molecular Weight: 113.116
• Mol file: 5325-93-9.mol

Synonyms:

Chemical Property of 2-cyanoethyl acetate

Chemical Property:

• Vapor Pressure: 0.222mmHg at 25°C
• Boiling Point: 207.8°C at 760 mmHg
• Flash Point: 86.4°C
• Density: 1.047g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-cyanoethyl acetate

There total 7 articles about 2-cyanoethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

acetic anhydride (108-24-7) + 3-Hydroxypropionitrile (109-78-4) → 3-acetoxy-propionitrile (5325-93-9)

Guidance literature:

With pyridine; for 24h;

DOI:10.1021/jp000227g

Reference yield:

2-cyanoethyl 2-bromoacetate (89322-55-4) → 3-acetoxy-propionitrile (5325-93-9)

Guidance literature:

With zinc; In tetrahydrofuran; Reflux;

DOI:10.1021/acs.joc.9b01001

Reference yield:

acetyl chloride (75-36-5) + 3-Hydroxypropionitrile (109-78-4) → 3-acetoxy-propionitrile (5325-93-9)

Guidance literature:

DOI:10.1039/P29770001914

upstream raw materials:

acetic anhydride

3-Hydroxypropionitrile

acetyl chloride

Ketene

Downstream raw materials:

acrylic acid

chloropropionic acid

acrylonitrile

acetic acid

Refernces

• 1、 Javaid et al.. "". . p. 596. Retrieved 1968.
• 2、 Jarikov, Viktor V.,Nikolaitchik, Alexandre V.,Neckers, Douglas C.. "Photochemistry and photophysics of (p-benzoylphenyl)diphenylmethyl and (p-benzoylphenyl)bis(4-tert-butylphenyl)methyl radicals in different solvents". . p. 5131 - 5140. Retrieved 2007/10/03.
• 3、 Chuchani, Gabriel,Martin, Ignacio,Hernandez, Jose A. A.,Rotinov, Alexandra,Fraile, German,Bigley, David B.. "Effects of Polar β Substituents in the Gas-Phase Pyrolysis of Ethyl Acetate Esters". . p. 944 - 948. Retrieved 2007/10/02.