Technology Process of Thallium, dichlorophenyl-
There total 4 articles about Thallium, dichlorophenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
P(C6H5)3;
In
dichloromethane;
(N2); addn. of triphenylphosphine to the soln. and stirring at 25 °C for 3 h;; solvent removal under reduced pressure; chromy. (TLC, petroleum spirit/CH2Cl2/Et2O); crystn. by slow evapn.; elem. anal.;
DOI:10.1016/0022-328X(88)80644-2
- Guidance literature:
-
In
chloroform;
room temp.;
- Guidance literature:
-
In
water;
thallic chloride in H2O was refluxed with phenylboronic acid, giving a product after 1 min; the product was filtered off, washed with small amt. of cold water, recrystd. from MeOH and dried;
