Disulfide, butyl phenyl

Base Information

• Chemical Name: Disulfide, butyl phenyl
• CAS No.: 20129-23-1
• Molecular Formula: C10H14S2
• Molecular Weight: 198.353
• DSSTox Substance ID: DTXSID40472828
• Nikkaji Number: J598.389D
• Wikidata: Q82301998
• Mol file: 20129-23-1.mol

Synonyms:Disulfide, butyl phenyl;butyl phenyl disulfide;butyldisulfanyl-benzene;20129-23-1;(butyldisulfanyl)benzene;SCHEMBL576770;DTXSID40472828

Chemical Property of Disulfide, butyl phenyl

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 198.05369279
• Heavy Atom Count: 12
• Complexity: 98

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCSSC1=CC=CC=C1

Technology Process of Disulfide, butyl phenyl

There total 35 articles about Disulfide, butyl phenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

thiophenol (108-98-5) + 5-(n-butylthio)-1,3-dimethyl-5-(4'-methoxybenzyl)barbituric acid (114657-01-1) → butyl phenyl disulfide (20129-23-1)

Guidance literature:

With pyridine; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4039(00)95570-9

Reference yield: 99.0%

thiophenol (108-98-5) + 5-(n-butylthio)-1,3-dimethyl-5-(4'-methoxybenzyl)barbituric acid (114657-01-1) → butyl phenyl disulfide (20129-23-1) + 5-(4-methoxybenzyl)-1,3-dimethylpyrimidine-2,4,6(1H,3H,5H)-trione (114656-99-4)

Guidance literature:

With pyridine; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4020(01)85957-3

Reference yield: 96.0%

n-butanethiol (109-79-5) + diphenyldisulfane (882-33-7) → butyl phenyl disulfide (20129-23-1)

Guidance literature:

With tetrabutyl-ammonium chloride; In acetonitrile; Ambient temperature; electrooxidation;

DOI:10.1080/00397919308011263

upstream raw materials:

n-butylsulfenyl chloride

thiophenol

n-butanethiol

benzenesulfenyl chloride

Downstream raw materials:

butane-1-thiosulfinic acid S-phenyl ester

(8-TB-5-22)-8-butylsulfanyl-8-phenyl-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole

dibutyl disulfide

diphenyldisulfane

Refernces

• 1、 Strehl, Julia,Hilt, Gerhard. "Synthesis of Symmetrical and Unsymmetrical Thiosulfonates from Disulfides through Electrochemically Induced Disulfide Bond Metathesis and Site-Selective Oxidation". supporting information. . Retrieved 2021/10/14.
• 2、 Soleiman-Beigi,Arzehgar. "A Novel Method for the Direct Synthesis of Symmetrical and Unsymmetrical Sulfides and Disulfides from Aryl Halides and Ethyl Potassium Xanthogenate". supporting information. p. 986 - 992. Retrieved 2018/02/09.