cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide

Base Information

• Chemical Name: cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide
• CAS No.: 41316-46-5
• Molecular Formula: C₂₀H₂₄N₄O₂
• Molecular Weight: 352.436
• Mol file: 41316-46-5.mol

Synonyms:

Chemical Property of cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide

There total 3 articles about cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromocyclohexane (108-85-0) → cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide (41316-46-5)

Guidance literature:

Multi-step reaction with 2 steps

1: alcohol; hydrazine hydrate / 140 °C / im Rohr

2: diethyl ether

With diethyl ether; ethanol; hydrazine hydrate;

Reference yield:

cyclohexylhydrazine (6498-34-6) + phenyl isocyanate (103-71-9) → cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide (41316-46-5) + 2-cyclohexyl-4-phenyl semicarbazide (856071-86-8)

Guidance literature:

With diethyl ether;

Reference yield:

→ cyclohexyl-hydrazine-N,N'-dicarboxylic acid dianilide (41316-46-5)

Guidance literature:

1-Cyclohexyl-4-phenylsemicarbazid, Phenylisocyanat;

DOI:10.1021/jo00961a024

upstream raw materials:

cyclohexylhydrazine

phenyl isocyanate

1-bromocyclohexane